Synthesis And Characterization of 5-(Mercapto-1,3,4Thiadiazole-2yl)α,α-Diphenyl Methanol From Benzilic Acid
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Abstract
5-(mercapto-1,3,4-thiadiazole-2yl)α,α-(diphenyl)methanol have been synthesized by ring closer of potassium xanthate[which have been prepared by reaction of benzilic acid hydrazide with carbon disulphide in potassium hydroxide] using conc.sulphuric acid at (0-5)°C scheme(I). Their characterization was carried out from T.L.C, M.P, FT.IR and 1H-NMR.
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Synthesis And Characterization of 5-(Mercapto-1,3,4Thiadiazole-2yl)α,α-Diphenyl Methanol From Benzilic Acid. (2017). Ibn AL-Haitham Journal For Pure and Applied Sciences, 26(1), 185-192. https://jih.uobaghdad.edu.iq/index.php/j/article/view/524
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Chemistry
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How to Cite
Synthesis And Characterization of 5-(Mercapto-1,3,4Thiadiazole-2yl)α,α-Diphenyl Methanol From Benzilic Acid. (2017). Ibn AL-Haitham Journal For Pure and Applied Sciences, 26(1), 185-192. https://jih.uobaghdad.edu.iq/index.php/j/article/view/524