Effect of Annealing Temperature on the Structural Characteristics of(Sb203) Compound.

Abstract

The crystal structure and unit cell dimensions of the (S03) compound have  been determined by employing the principles of crystallography.

The X-Ray diffraction spectra of (Sb203) which recorded as a function  of   different  annealing  temperatures  (100,150,200  and

250)±5c and for durations (0.5  hr,

0

1hr, l.Shr and 2hr), showed a

noticeable improvement, a decreasing in the unit cell dimensions and

an increasing in the number of diffraction spectra.

Indexing of diffraction spectra and refinement of  unit cell

dimensions showed that the compound (Sb203)  which is a  cubic system are (a=ll.271A)   before annealing, and (a= ll.207A)  after annealing at 250±5c for (2hr).