Effect of the Synthesis Time on Structural Properties of Copper Oxide

Authors

karrar alsoltani Department of Physics, College of Education for Pure Science Ibn Al-Haitham, University of Baghdad
Khalid H. Harbbi Department of Physics, College of Education for Pure Science Ibn Al-Haitham, University of Baghdad

DOI:

https://doi.org/10.30526/36.2.3024

Keywords:

CuO, Originpro, XRD, halder-wagner, size-strain plot

Abstract

The structural properties of the CuO nanopowder oxide prepared reflux technique
without any templates or surfactant, using copper nitrate hydrate (Cu(NO)3 3H2O) in deionized
water with aqueous ammonia solution are reported. The Xrd analysis data and processing in origin
pro program used to get FWHM and integral width to study the effect of different synthesis times
was studied on the structural properties. It was found that values of crystal sizes are 17.274nm,
17.746nm, and 18.560nm, the size of nanoparticles is determined by Halder-Wagner, and 15.796
nm, 15.851nm, and 16.52nm, were calculated by Size-Strain Plot (SSP) method. The Sample was
considered to determine physical and microstructural parameters such as internal strain,
dislocations density, surface area, and the number of unit cells and then to compare the results.

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