Synthesis And Imidization Of Disuccinamic Acid As Polyvinyl Alcohol-Composite Polymer

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Zakaria H. Aiube
Fadhel S. Matty
Hiba A. Ghani Al-zaidi

Abstract

  Two arylenedisuccinamic acids, namely 1,4-phenylene-disuccinamic acid and 4,4'biphenyl-disuccinamic acid were prepared from the reaction of two moles of succinic anhydride with one mole of 1,4-phenylenediamine dihydrochloride and beinzidine respectively.Dehydration of arylenedisuccinamic acid in the pressence of polyvinyl alcohol (PVA) and catalytic amount of concentrated.H2SO4,gives N,N'-arylenedisuccinimidesPVAcomposite polymers. Dehydration of arylenedisuccinamic acid (without PVA) in the pressence of catalytic amount of conc. H2SO4 gives N,N'-arylenedisuccinimides. Arylenedisuccinamic acid and arylenedisuccinimides characterized by CHN-analysis,FT.IR and 1H,C13-NMR.Spectral analysis

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How to Cite
Aiube, Z. H., Matty, F. S., & Al-zaidi, H. A. G. (2017). Synthesis And Imidization Of Disuccinamic Acid As Polyvinyl Alcohol-Composite Polymer. Ibn AL-Haitham Journal For Pure and Applied Sciences, 27(2), 211–219. Retrieved from https://jih.uobaghdad.edu.iq/index.php/j/article/view/345
Section
Chemistry