Effect of Zinc Additive and Annealing on Dielectric Characteristics of the PSCCO Compound

shatha hashim mahdi; Naba  F. Hamady; Demiral  Akbar

doi:10.30526/38.1.3917

Authors

Shatha. H. Mahdi Department of Physics, College of Education for Pure Science (Ibn Al-Haitham), University of Baghdad, Baghdad, Iraq. https://orcid.org/0000-0001-9755-5544
Naba F. Hamady Department of Physics, College of Education for Pure Science (Ibn Al-Haitham), University of Baghdad, Baghdad, Iraq. https://orcid.org/0000-0001-9755-5544
Demiral Akbar Department of Physics, OSTİM Technical University, Ankara, Turkey. https://orcid.org/0000-0002-2102-1885

DOI:

https://doi.org/10.30526/38.1.3917

Keywords:

alternating electrical conductivity, composite, superconductivity, Ceramic, dielectric properties, Electric Capacitance

Abstract

The ceramic PSCCO (PbSr₂Ca₂Cu₃O) and (PbSr₂Ca₂Cu_2.4Zn_0.6O) compounds were prepared using high-purity oxides (x=0 and0.6%) via solid reaction. The samples were then pressed into tablets with 1.5 cm diameter, at 5.4MPa for two minutes and sintered at 850°C for 24 hours. AFM was used to study the surface structure. It showed a stable improvement in the crystallization of the model surfaces. As a result of the chemical reaction between the raw materials, the granules united with each other, increasing their size. At a frequency range of 50-10⁶ Hz, regarding the dielectric properties, including the dielectric constant, and dielectric loss factor, at room temperature, it measured electrical conductivity and electrical resistance as a function of frequency in the range from 50 to10⁶Hz, Measurements of the ceramic composite model PSCCO (PbSr₂Ca₂Cu₃O) plus (PbSr₂Ca₂Cu_2.4Zn_0.6O) showed dielectric constant (11.23 and 10.30), while also measuring the loss angle shadow and alternating conductivity. The following parameters were measured for two models at a frequency range of 50-10⁶ Hz: dielectric loss factor (7.76 and 9.45), tangent loss tangent (tanδ) (0.69 and 0.91), and alternating electrical conductivity (σ_a.c). The dielectric constant values for both models were 11.23 and 12.43. The insulating properties showed good stability with temperature within the range of room temperature to 200°C.and 13.71 for the base compound PbSr₂Ca₂Cu₃O, at different temperatures, the dielectric constant of compound PbSr₂Ca₂Cu_2.4Zn_0.6O was measured to be 10.3, 11.15, and 12.06, indicating its potential use at high temperatures.

Author Biographies

Shatha. H. Mahdi , Department of Physics, College of Education for Pure Science (Ibn Al-Haitham), University of Baghdad, Baghdad, Iraq.

Department of Physics, College of Education for Pure Science Ibn Al-Haitham, University of Baghdad, Baghdad, Iraq.
Naba F. Hamady, Department of Physics, College of Education for Pure Science (Ibn Al-Haitham), University of Baghdad, Baghdad, Iraq.

.
Demiral Akbar, Department of Physics, OSTİM Technical University, Ankara, Turkey.

Department of Physics, OSTİM Technical University, Ankara, Turkey.

References

Iyo A, Tanaka Y, Kito H, Kodama Y, Shirage PM, Shivagan DD. Watanabe. Condensed matter: Electronic structure and electrical, magnetic, and optical properties vs n Relationship for Multilayered High-Tc Superconductors. J Physics Procedia. 2007;76(9):94711-94711. https://doi.org/10.1143/JPSJ.76.094711

Alborzi Z, Daadmehr V. Isovalent Substitution Effects of Arsenic on Structural and Electrical Properties of Iron-Based Superconductor NdFeAsO 0.8 F 0.2. J Supercond. Nov Magn .2020; 33:387-396.‏ https://doi.org/10.48550/arXiv.1901.00797

Khan MI, Bhatti KA, Qindeel R, Alonizan N, Althobaiti HS. Characterizations of multilayer ZnO thin films deposited by sol-gel spin coating technique. Results Phys. 2017; 7(4): 651-655.

https://doi.org/10.1016/j.rinp.2016.12.029

Sultana R, Rani P, Hafiz AK, Goyal R, Awana S. An Intercomparison of the Upper Critical Fields (HC2) of Different Superconductors—YBa 2Cu3O7, MgB2, NdFeAsO 0. 8 F0.2, FeSe0.5 Te0.5 and Nb 2 PdS5. J Supercond. Nov Magn. 2016; 29: 1399-1404. DOI:10.1007/s10948-016-3507-1

Hussein BH, Mahdi SH, Makki S A, Al-Maiyaly BK. Synthesis and Study the Structure, electrical and optical properties of Bi2-xCdxSr2Ca2Cu3O10+ δ thin film Superconductors. Energy Procedia. 2019; 157:100-110. https://doi.org/10.1016/j.egypro.2018.11.169

Jasim KA, Mohammed LA. The partial substitution of copper with nickel oxide on the Structural and electrical properties of HgBa2 Ca2 Cu3xNix O8+ δ superconducting compound. Journal of Physics: Conference Series. IOP Publishing. 2018; 1003(1): 012071.https://iopscience.iop.org/article /10.1088/1742-6596/1003/1/012071

Mohammed LA, Jasim KA. Improvement the Superconducting properties of TlBa2 Ca2 Cu3xNix O 9-δ superconducting compound by partial substitution of copper with nickel oxide on the. Energy Procedia. 2019; 157:135-142. https://doi.org/10.1016/j.egypro.2018.11.173

Jobayr MR, Mahdi SH, Salman EM, Jasim KA. Effect of antimony on characteristics of HgBa 2 CaCu 2-x Sb x O 8+ δ superconducting. J Ovonic Res. 2022; 18(3): 357-371. https://doi.org/10.15251/JOR.2022.183.357

Beena P, Jayanna HS. Dielectric studies and AC conductivity of piezoelectric barium titanate ceramic polymer composites. Polym. Polym. Compos. 2019; 27(9):619-625. https://doi.org/10.1177/0967391119856140

Haider S, Kareem A. Effect of Partial Substitution of Lanthanum (La) on the Structural and Electric Properties of Bi2Sr2Ca2Cu3xLaxO10+δ. Ibn Al-Haitham J for Pure & Appl Sci.2017; 30( 3) 35-43 .https://doi.org/10.30526/30.3.1600

Fouad WA, Kareem AJ. Preparation and study of structural properties, transition temperature and thermal conductivity of the HgBa2Ca2Cu3O8+δ and HgBa2CaCu2O6+δ Nanomaterial compounds. AIP Conf. Proc. 2023;3018, 020055-1 - 020055-7. https://doi.org/10.1063/5.0172303

Ali MA, Jasim KA. Studying the Influence of fast neutron irradiation on properties of Bi2-x Pbx Sr2 Ca2 Cu3-y Niy O2n+ 4+ δ superconducting system. Energy Procedia. 2019; 157:143-149. https://doi.org/ 10.1016/j.egypro.2018.11.174

Jasim KA. Structure and electrical properties of lanthanum doped Bi_2Sr_2Ca_ {2-x} La_xCu_3O_ {10+delta} superconductor. Turk J Phys. 2012; 36(2):245-251. https://doi.org/10. 3906/fiz-1105-12

Mumtaz M, Khan NA, Khan S. Study of Dielectric Properties of Oxygen-Postannealed Cu0.5Ti0.5Ba2Ca2 (Cu3-yMy)O10-δ Superconductor. IEEE Trans on App Supercond J . 2013; 23(2):1-8. http://dx.doi.org/10.1109/TASC.2013.2245505

Tawfiq LN, Hassan MA. Estimate the Effect of Rainwaters in Contaminated Soil by Using Simulink Technique. In Journal of Physics: Conference Series. IOP Publishing. 2018;1003(1):1-6. https://iopscience.iop.org/article/10.1088/1742-6596/1003/1/012057

Solov’ev AL, Dmitriev VM. Fluctuation conductivity and pseudogap in YBCO high-temperature superconductors. Low tem phys. 2009;35(3):169-197. https://doi.org/10.1063/1.3081150

Haider HM, Jasim KA. Effect of Composition and Dielectric Properties for (YBCO) superconductor compound in different preparation methods Ibn al-Haitham j pure appl sci. 2020;33(1):17-30. https://doi.org/10.30526/33.1.2372

Younis A, Khan N A, Bajwa N U. Dielectric properties of Cu0. 5Tl0. 5Ba2Ca3Cu4− yZnyO12− δ (y= 0, 3) superconductors. J Korean Phys Soc. 2010;57(6) 1437-1443. https://doi.org/10.1063/1.3677234

Mahdi ShH , Mohammed LA, Fadhil RN, Hussein BH. Fabrication and study of characteristics of HgSr 2 Ca n-1 Cu n O δ+10, (n =1,2 and 3) thin films superconducting. Dig. J Nanomater Biostructures. 2023; 18(2):579-590. http://dx.doi.org/10.15251/DJNB.2023. 182.579

Ahmad NA, Ali AD, Mahdi SH. Studying the effect partial Ni2O3 nano-particles compensation on the properties of the compound Bi2 Sr2-xYx Ca2 Cu3-y Niy O10+δ superconductors. J Ovonic Res., 2023;19(4):463–469. https://doi.org/10.15251/JOR.2023.194.463

Hassan AT, Ghazala YH, Bushra AA. Superconducting Properties of the (Bi0.8Pb0.2)2(Sr0.9Ba0.1)2 Ca2Cu3-x Nix O10+? System. Baghdad Sci J.2011;8(2):1-10. https://doi.org/10.21123 /bsj.2011.8.2.607-612

Jassim KA, Thejeel MA, Salman EM, Mahdi SH. Study characteristics of (epoxy–bentonite doped) composite materials. Energy Procedia. 2017; 119: 670-679. https://doi.org/10.1016/j.egypro. 2017.07.094

Güzin P, Gülben T, Fatih B. Electrical properties of two-armed poly(Ɛ-CL-co-BMA) composites filled with bentonite. J Polym Res .2020;27(156):1-13 https://doi.org/10.1007/s10965-020-02119-z

Mahdi SH, Jassim WH, Hamad IA, Jasima KA. Epoxy/silicone rubber blends for voltage insulators and capacitors applications. Energy Procedia. 2017; 119: 501-506. https://doi.org/10.1016/j.egypro. 2017.07.059

Gülben T, Nedim G. Investigation of Dielectric Properties of Graphene Filled Starch Films in Wide Frequency Range Grafen Katkılı Nişasta Filmlerinin Dielektrik Özelliklerinin Geniş Frekans Aralığında İncelenmesi. Iğdır Üniversitesi Fen Bilimleri Enstitüsü Dergisi. J Inst Sci Technol 2021;11(2):1393-1401.https://doi.org/10.21597/jist.830255

Narang SB, Kaur D, Pubby K. Frequency and temperature dependence of dielectric and electric properties of BaSmTiO with structural analysis. J Mater Sci Pol.. 2015;33(2):268-277. https://doi.org/10.1515/msp-2015-0034

Fadhil RN, Mahdie SH, Jasim KA, Shaban AH. Effect Partial Substitution of Calcium by Cadmium on Dielectrically Properties of Li0.4Cd0.6Ba2Ca2Cu3O10+δ System. Mater Sci Forum. 2022; 1050:35-40. https://doi.org/10.4028/www.scientific.net/MSF.1050.35

Weijie Z, Yutie G, Hairong L, Jing H, Qiongxin L, Wei W, Xiaoyuan Q, Ming J, Jiuxiao S. Thermo‐responsive dielectric pulse in poly(vinylidene fluoride)/polyethylene glycol fibrous Mats Polym Eng Sci. 2022;62(11):3662-3671. https://doi.org/10.1002/pen.26135

Kareem AJ, Akram HT, Auday HS. The Effective of Pressure on the Physical Proprieties of Y2Ba4Cu7O15 Superconductor Materials Science Forum. 2022; 1050: 3-8. https://doi.org/10.4028/ www. scientific.net/MSF.1050.3

Ramajo LA, Cristóbal AA, Botta PM, Porto JM, Reboredo MM, Castro MS. Dielectric and magnetic response of Fe3O4/epoxy composites. Compos. Part A: Appl Sci Manuf. 2009;40(4):388-393. https://doi.org/10.1016/j.compositesa.2008.12.017