Synthesis, Characterization Of New Schiff Base And Some Metal Complexes Derived From Glyoxylic Acid And O-Phenylenediamine
Keywords:
Synthesis, Characterization, Schiff base, glyoxylic acid, O-phenylenediamine and metal ionsAbstract
The new Schiff base, namely (2-Amino-phenylimino)-acetic acid (L) was prepared
from condensation of glyoxylic acid with o-phenylene diamine. The structure (L) was
characterized by, IR,
1
H,
13
C-NMR and CHN analysis. Metal complexes of the ligand (L)
were synthesized and their structures were characterized by Atomic absorption, IR and UV-Visible spectra, molar conductivity, magnetic moment and molar ratio determination (Co
+2
,
Cd
+2
) complexes. All complexes showed octahedral geometries.